Chemistry – Mykhailiuk Research Site

Mykhailiuk Research Site
Organic synthesis for drug discovery

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Chemistry

The synthesis

In situ generation of CF3CHN2

I do not even know what is that

Yellow synthesis

A looot of something orange

Setting up the photo-redox catalysis

Making fluorinated pyrazoles

Purification of the product by the sublimation under vacuum

Crystalls for X-Ray

Tubes for photochemistry 20 mg scale

Photochemistry 1

Photochemistry 2

Photochemistry 3

Photochemistry 4

Column chromatography

Generation of CF2HCHN2 in situ

Derivatives of L Proline

Chaos in the lab 1

pH metrics

Fumehood

Chaos in the lab 2

This is clean

Liophiliser

Lab, the lab

Chemical flasks

Balls and sticks model of Proline

Reactor for photochemistry in flow

Reactors for photochemistry in flow

Photochemistry 50 g scale

Photochemical 2+2 cycloaddition in NMR tube

Fractions after a column chromatography

Lab mouses 1

Lab mouses 2

Lab mouses 3

Inside the flask

Almost a rainbow

Designed by Salvador Dalí

This compound might be very pure

Almost an orange

Photochemistry 20 g scale

NMR tubes

Fractions after a column chromatography 2

Crystallization

The pink synthesis

Chemical beauty 2

Chaos in the lab 3

Chaos in the lab 4

DMSO-d6

Ion exchange chromatography

Building block from Enamine

Proline analogue

Proline analogue 2

Proline analogues

Chaos in the lab 5

Column chromatography 2

Fumehood 2

1 kg of 24 methanoproline

2-CF3 azeridine

3-CF3 azetidine

Bubbles

Chemical beauty 3

Chemical beauty 4

Chemical beauty

Distillation

Column chromatography 2

Column chromatography the rainbow

Funny synthesis

In-flow reactor

Hydrogenation over Pd-C

Our SpaceX mission is ready to go to Mars

Reactor for photochemistry

Something went wrong

The dill in the flask

Preparation for the synthesis of propellane

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